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| 毛细柱——微电子捕获气相色谱法测定水中氯仿、四氯化碳 | |
| 引用本文： | 许瑛华,杜达安. 毛细柱——微电子捕获气相色谱法测定水中氯仿、四氯化碳[J]. 卫生研究, 2002, 31(2): 124-125 |
| 作者姓名： | 许瑛华 杜达安 |
| 作者单位： | 广东省疾病预防控制中心,广州,510300 |
| 摘 要： | 毛细柱－微电子捕获气相色谱法水中氯仿，四氯化碳，其线性范围得到扩延，氯仿浓度在0－10μg/L范围内，相关系数r=0.9910，回归方程Y＝1．959X＋4．816，最低检出学为0．1032μg/L，四氯化碳浓度在0－1μg/L，范围内，相关系数r=0.9970，回归方程Y＝3．947X＋42．579，最低检出浓度为0．01219μg/L。同时，本方法简化了操作过程，方法灵敏度得到较大提高，并且准确度和精密度均符合检测要求。 |
| 关 键 词： | 顶空法 氯仿 四氯化碳 饮用水 毛细柱－微电子捕获 气相色谱法 测定 |
| 文章编号： | 1000-8020(2002)02-0124-02 |
| 修稿时间： | 2001-03-02 |
Determination of chloroform and tetrachloro|methane in water with capillary column-μECD |
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| Xu Yinghua,Du Daan Disease Prevention and Control Center of Guangdong Province,Guangzhou ,China. Determination of chloroform and tetrachloro|methane in water with capillary column-μECD[J]. Journal of hygiene research, 2002, 31(2): 124-125 | |
| Authors: | Xu Yinghua Du Daan Disease Prevention Control Center of Guangdong Province Guangzhou China |
| Affiliation: | Disease Prevention and Control Center of Guangdong Province, Guangzhou 510300, China. |
| Abstract: | The method of determination of chloroform and tetrachloro-methane in water with capillary column-microECD had better and wider linear range and lower detection limit. At the range of 0-10 micrograms/L chloroform and 0-1 microgram/L tetrachloro-methane, the regression equation were calculated as Y = 1.959X + 4.816 (r = 0.9910) and Y = 3.947X + 42.58 (r = 0.9970). The lowest detection limit were 0.1032 microgram/L chloroform and 0.01219 microgram/L tetrachloro-methane. This method not only simplified the operating processes, but also increase the sensitivity, and reavled better precision and accuracy. |
| Keywords: | headspace chloroform tetrachloro|methane water |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |