气相色谱法测定化妆品中氮芥 |
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引用本文: | 张剑峰,高建,刘静晶,张毅,高源,仲伟明. 气相色谱法测定化妆品中氮芥[J]. 中国卫生工程学, 2010, 0(1): 47-48 |
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作者姓名: | 张剑峰 高建 刘静晶 张毅 高源 仲伟明 |
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作者单位: | 黑龙江省疾病预防控制中心,黑龙江哈尔滨150030 |
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摘 要: | 目的建立用气相色谱测定化妆品中氮芥的方法。方法化妆品中的氮芥用萃取法进行富集,用具有氢火焰离子化检测器的气相色谱仪测定。结果该方法RSD均10%,加标回收率为85.5%~105.2%,最低检出线为0.5μg/g。结论该方法符合试验要求,具有操作简单、快速的特点,适于化妆品中氮芥的测定。
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关 键 词: | 化妆品 气相色谱 氮芥 |
Determination of Chlormethine in Cosmetic by Gas Chromatography |
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Affiliation: | ZHANG Jian -feng, GAO Jian, LIU Jing -jing, et al. (Heilong jiang Center for Disease Confrol and Prevention, Harbin Heilongjiang 150030, China.) |
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Abstract: | Objective To develop a method for determination of chlormethine in cosmetic.Methods Chlormethine in cosmetic was enriched by extraction method and determined with FID detector.Results The relative standard deviation was less than 10%,the recovery rate was 85.5%-105.2%,the detection limit was 0.5 μg/g.Conclusion The method is rapid,easy to operate.It fits to determine chlormethine in cosmetic. |
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Keywords: | Cosmetic Gas chromatography Chlormethine |
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