| 气相色谱法检测中药材中多种农药残留 |
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| 引用本文： | 秦岩,孙立华,吴爱英,祝波,李义鸽. 气相色谱法检测中药材中多种农药残留[J]. 中国药师, 2011, 14(10): 1436-1439 |
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| 作者姓名： | 秦岩 孙立华 吴爱英 祝波 李义鸽 |
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| 作者单位： | 1. 青岛药品检验所 山东青岛266071
2. 济宁医学院药学分院 |
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| 基金项目： | “十一五”国家科技支撑计划项目(编号:2008BAI55B02) |
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| 摘 要： | 目的:建立87种中药材中有机氯类、拟除虫菊酯类等多种农药残留的GC-ECD测定方法。方法:针对不同样品,选用DB-1701毛细管柱,通过柱程序升温,对多种农药进行同时检测。结果:各种农药在2～2 000μg·L-1浓度范围内与峰面积呈良好的线性关系,检出限为0.094 6～14.150 9 Pg。结论:本方法快速、简便、准确。
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| 关 键 词： | 农药残留量 气相色谱 电子捕获检测器 |
| 收稿时间： | 2011-07-29 |
| 修稿时间： | 2011-08-22 |
Determination of Pesticide Residues in Traditional Chinese Medicines by Gas Chromatography |
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| Qin Yan,Sun Lihu,Wu Aiying,Zhu Bo and Li Yige. Determination of Pesticide Residues in Traditional Chinese Medicines by Gas Chromatography[J]. China Pharmacist, 2011, 14(10): 1436-1439 |
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| Authors: | Qin Yan Sun Lihu Wu Aiying Zhu Bo Li Yige |
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| Affiliation: | Qingdao Institute for Drug Control, Shandong Qingdao 266071, China;Qingdao Institute for Drug Control, Shandong Qingdao 266071, China;Qingdao Institute for Drug Control, Shandong Qingdao 266071, China;Qingdao Institute for Drug Control, Shandong Qingdao 266071, China;Jining Medical University |
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| Abstract: | Objective： To determine pesticide residues of organchlorines and pyethroids in 87 kinds of traditional Chinese medi- cines by gas chromatography with electron capture detector. Method： The pesticide residues in different samples were extracted and separated by DB-1701 column with temperature programming. Result： Many sorts of pesticides could be separated perfectly. The standard curves all showed good linearity over the concentration range of 2-2 000 μg · L^-1 and the detection limit of the pesticides was 0. 094 6-14. 150 9 pg. Conclusion： The method is rapid, simple and accurate. |
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| Keywords: | Pesticide residue Gas chromatography Electron capture detector |
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