| 四味生津颗粒的质量标准研究 |
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| 引用本文： | 朱三甫,秦霞,李成网.四味生津颗粒的质量标准研究[J].中国药房,2012(27):2560-2562. |
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| 作者姓名： | 朱三甫 秦霞 李成网 |
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| 作者单位： | 淮南联合大学化工系,安徽淮南232038 |
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| 摘 要： | 目的:建立四味生津颗粒的质量标准。方法:采用薄层色谱(TLC)法对方中甘草、白芍、知母、生地黄进行定性鉴别;高效液相色谱法测定方中芍药苷含量。结果:TLC斑点清晰、分离度好,阴性对照无干扰;芍药苷进样量在0.6344～3.1720μg范围内与峰面积积分值呈良好的线性关系(r=0.9990,n=5),平均回收率为97.60%,RSD=1.83%(n=6)。结论:所建标准可用于四味生津颗粒的质量控制。
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| 关 键 词： | 四味生津颗粒 质量标准 薄层色谱法 高效液相色谱法 芍药苷 |
Study on the Quality Standard of Siwei Shengjin Granules |
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| ZHU San-fu,QIN Xia,LI Cheng-wang.Study on the Quality Standard of Siwei Shengjin Granules[J].China Pharmacy,2012(27):2560-2562. |
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| Authors: | ZHU San-fu QIN Xia LI Cheng-wang |
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| Institution: | (Dept. of Chemical Engineering, Huainan Union University,Anhui Huainan 232038, China) |
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| Abstract: | OBJECTIVE： To establish the quality standard of Siwei shengjin granule. METHODS： Glycyrrhiza, Paeonia sterni- ana, Anemarrhena asphodeloides and Radix Rehmanniae were identified by TLC. HPLC method was used to determine the content of paeoniflorin. RESULTS： TLC spots were clear and well-separated without interference from negative control. The linear range of paeoniflorin was 0.634 4-3.172 0 μg（r=0.999 0, n=5）. The average recovery was 97.60% （RSD=1.83%, n=6）. CONCLU- SION： Established standard can be used for the quality control of Siwei shengjin granules. |
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| Keywords: | Siwei shengjin granules Quality standard TLC HPLC Paeoniflorin |
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