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| 尾叶香茶菜的高效液相指纹图谱研究 | |
| 引用本文： | 朱晓红,王强,杨丽霞,臧树良. 尾叶香茶菜的高效液相指纹图谱研究[J]. 解放军药学学报, 2008, 24(4): 326-329 |
| 作者姓名： | 朱晓红 王强 杨丽霞 臧树良 |
| 作者单位： | 华东师范大学,化学系,上海,200062;解放军第202医院,辽宁,沈阳,100003;解放军第202医院,辽宁,沈阳,100003;辽宁大学化学科学与工程技术院,辽宁,沈阳,110036 |
| 摘 要： | 目的采用反相高效液相色谱法建立尾叶香茶菜的指纹图谱。方法采用Diamonsil C18色谱柱（5μm，250mm×4．6mm）；流动相为乙腈-水（23：77）；流速1．0ml／min；柱温为25℃；检测波长为230nm。结果建立了尾叶香茶菜的高效液相色谱指纹图谱。8批尾叶香茶菜指纹图谱相似度≥0．9435。结论采用HPLC指纹图谱检测技术可有效控制尾叶香茶菜的质量。 |
| 关 键 词： | 尾叶香茶菜 指纹图谱 HPLC |
Studies on Fingerprint Chromatograms of Rabdosia excisa (Maxim.) Hara by HPLC |
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| ZHU Xiao-Hong,WANG Qiang,YANG Li-Xia,ZANG Shu-Liang. Studies on Fingerprint Chromatograms of Rabdosia excisa (Maxim.) Hara by HPLC[J]. Pharmaceutical Journal of Chinese People's Liberation Army, 2008, 24(4): 326-329 | |
| Authors: | ZHU Xiao-Hong WANG Qiang YANG Li-Xia ZANG Shu-Liang |
| Affiliation: | ZHU Xiao-Hong, WANG Qiang, YANG Li-Xia, ZANG Shu-Liang (1.Department of Chemistry, East Normal University, Shanghai 200062 China;2.No. 202 Hospital of PLA,Shenyang 110003 ,Liaoning China;3.Department of Chemistry, Liaoning University,Shenyang 110036, Liaoning China) |
| Abstract: | Aim To study and establish the fingerprint of raw Rabdosia excisa （ Maxim. ） Hara by RP-HPLC.Methods The chromatographic conditions were as follows：a Diamonsil C18 column was used; the mobile phase was composed of acetontrile and water（ V： V = 23： 77 ） ; the flow rate was 1.0mL/min; the column temperature was 25℃ and the detection wavelength was set at 230nm. Results The fingerprint of raw Rabdosia excisa （ Maxim. ） Hara was established. The similarity of 8 batches of raw Rabdosia excisa （ Maxim. ） Hara was not lower than 0.943 5. Conclusion The quality of raw Rabdosia excisa （ Maxim. ） Hara can be controlled effectively by HPLC fingerprint. |
| Keywords: | HPLC |
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