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食盐中亚硝酸盐测定方法的研究
引用本文:刘友序,于秀玲. 食盐中亚硝酸盐测定方法的研究[J]. 口岸卫生控制, 2009, 14(1): 18-20
作者姓名:刘友序  于秀玲
作者单位:1. 天津出入境检验检疫局,天津,300456
2. 中盐制盐工程技术研究院,天津,300450
摘    要:
该文提出了食用盐中亚硝酸盐的测定方法。食盐中的亚硝酸盐在弱酸性条件下,与对a-氨基苯磺酸重氮化后,和N-1-盐酸萘己二胺偶合形成紫红色染料,在538nm的波长下,光度法测定。线性范围0mg/L-0.3mg/L,线性相关系数r=0.999x,检出限为0.14mg/kg的亚硝酸钠含量。

关 键 词:食盐  亚硝酸盐  分光光度法  重氮偶合反应

Research on nitrite determination in table salt
Liu Youxu,Yu Xiuling. Research on nitrite determination in table salt[J]. , 2009, 14(1): 18-20
Authors:Liu Youxu  Yu Xiuling
Affiliation:(Tianjin entry-exit inspection and quarantine bureau of the P.R. China(Tianjin,300456) Salts research institute China national salt industry corporation (Tianjin,300450))
Abstract:
The paper described analytic methods of nitrite in table salt. In weak acidic solution, nitrite diazoed with a-aminobenzene sulfonic acid, then couple with N-(1-Naphthyl)-ethylenediamine dihydrochloride, making into fuchsia dyestuff. The content of nitrite was determined by spectrophotometry under 538 nm wavelength. The detectable linear range is from 0 mg/L through 0.3 mg/L, the correlation coefficient R equals 0.999 x, the detection limit is 0.14 mg/kg.
Keywords:Table salt  nitrite spectrophotometry  diazo coupling reaction
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