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补肾强身胶囊中淫羊藿苷的含量测定
引用本文:龚玲,徐林,孙月华.补肾强身胶囊中淫羊藿苷的含量测定[J].北方药学,2014,0(6):1-2.
作者姓名:龚玲  徐林  孙月华
作者单位:贵州省安顺市食品药品检验所 安顺 561000;贵州省安顺市疾病预防控制中心 安顺 561000;安顺学院 安顺 561000
摘    要:采用高效液相色谱法测定补肾强身胶囊中淫羊藿苷的含量。以XB-C18为色谱柱,以乙腈-水(30∶70)为流动相,以270nm为检测波长,流速为1.0ml/min,柱温为30℃。淫羊藿苷在16.576-165.76ug/ml的浓度范围内线性关系良好,R^2=1,平均回收率为100.2%,RSD%为0.74%。该方法简便、快捷、准确,能有效地控制补肾强身胶囊的质量。

关 键 词:高效液相色谱法  补肾强身胶囊  淫羊藿苷

Determine the content of epimedium glycoside in the kidney and strength capsule
GONG Ling,XU Lin,SUN Yue-hua.Determine the content of epimedium glycoside in the kidney and strength capsule[J].BEIFANG YAOXUE,2014,0(6):1-2.
Authors:GONG Ling  XU Lin  SUN Yue-hua
Institution:1.Guizhou Anshun City Food and Drug Inspection Office ;2.Guizhou Anshun City Center for Disease Control and Prevention 3. Anshun College)
Abstract:Using high performance liquid chromatography (HPLC)method was developed for the determination of epimedium glycoside in kidney and strengthen the capsule content. For XB - C18 chromatographic column, with acetonitrile - water (30∶70)as mobile phase, detection wavelength for 270nm, the flow rate of 1.0 ml/min, column temperature 30℃. Epimedium glycoside in 16.576 to 165.76ug/ml concentration range inside sex good, R^2=1, the average recovery was 100.2%, RSD % to 0.74%. The method is simple, quick, accurate, and can effectively control the quality of the kidney and strengthening the capsule.
Keywords:High performance liquid chromatography  Kidney and strengthen the capsule  Epimedium glycoside
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