| UPLC-PDA同时测定藏药翼首草环烯醚萜苷和酚酸类10个化学成分的含量 |
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| 引用本文： | 唐策,文检,王静,赵可惠,范刚,孟宪丽,邹忠梅,张艺.UPLC-PDA同时测定藏药翼首草环烯醚萜苷和酚酸类10个化学成分的含量[J].中国中药杂志,2017,42(7):1234-1237. |
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| 作者姓名： | 唐策 文检 王静 赵可惠 范刚 孟宪丽 邹忠梅 张艺 |
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| 作者单位： | 成都中医药大学 民族医药学院, 四川 成都 611137,成都中医药大学 民族医药学院, 四川 成都 611137,成都中医药大学 民族医药学院, 四川 成都 611137,成都中医药大学 民族医药学院, 四川 成都 611137,成都中医药大学 民族医药学院, 四川 成都 611137,成都中医药大学 民族医药学院, 四川 成都 611137,中国医学科学院 北京协和医学院 药用植物研究所, 北京 100193,成都中医药大学 民族医药学院, 四川 成都 611137 |
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| 基金项目： | 国家自然科学基金面上项目（81274193）；四川省教育厅属高校科研创新团队建设计划项目（11TD004） |
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| 摘 要： | 建立超高效液相色谱法(UPLC-PDA)同时测定藏药翼首草环烯醚萜和酚酸类10个化学成分的含量。采用Acquity UPLC~R BEH C_(18)(2.1 mm×100 mm,1.7μm)色谱柱,流动相0.2%磷酸水(A)-乙腈(B),梯度洗脱,检测波长237,325 nm,流速0.4 mL·min~(-1),柱温30℃,进样量1μL。研究结果表明UPLC-PDA法定量分析翼首草10个化学成分在考察的范围内线性关系良好(r≥0.999 7);加样回收率为96.30%~103.0%(n=9),RSD为0.72%~2.9%(n=9)。所建立UPLC方法简便、准确、重复性好,可同时测定藏药翼首草中10个化学成分的含量。
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| 关 键 词： | 藏药 翼首草 UPLC-PDA 环烯醚萜 酚酸 含量测定 |
| 收稿时间： | 2016/11/1 0:00:00 |
Simultaneous determination of ten major compounds including iridoid glycosides and phenolic acids in Pterocephalus hookeri by UPLC-PDA |
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| TANG Ce,WEN Jian,WANG Jing,ZHAO Ke-hui,FAN Gang,MENG Xian-li,ZOU Zhong-mei and ZHANG Yi.Simultaneous determination of ten major compounds including iridoid glycosides and phenolic acids in Pterocephalus hookeri by UPLC-PDA[J].China Journal of Chinese Materia Medica,2017,42(7):1234-1237. |
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| Authors: | TANG Ce WEN Jian WANG Jing ZHAO Ke-hui FAN Gang MENG Xian-li ZOU Zhong-mei and ZHANG Yi |
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| Institution: | College of Ethnic Medicine, Chengdu University of Traditional Chinese Medicine, Chengdu 611137, China,College of Ethnic Medicine, Chengdu University of Traditional Chinese Medicine, Chengdu 611137, China,College of Ethnic Medicine, Chengdu University of Traditional Chinese Medicine, Chengdu 611137, China,College of Ethnic Medicine, Chengdu University of Traditional Chinese Medicine, Chengdu 611137, China,College of Ethnic Medicine, Chengdu University of Traditional Chinese Medicine, Chengdu 611137, China,College of Ethnic Medicine, Chengdu University of Traditional Chinese Medicine, Chengdu 611137, China,Institute of Mechcinal Plant Development, Chinese Acadeuy of Medical Scieuce and Peking Union Medical College, Beijing 100193, China and College of Ethnic Medicine, Chengdu University of Traditional Chinese Medicine, Chengdu 611137, China |
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| Abstract: | |
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| Keywords: | Tibetan medicine Pterocephalus hookeri UPLC-PDA iridoid glycoside phenolic acid content determination |
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