| 气相色谱法测定黑水缬草挥发油中乙酸龙脑酯的含量 |
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| 引用本文： | 霍金海,都晓伟,孙晖,陈雪英.气相色谱法测定黑水缬草挥发油中乙酸龙脑酯的含量[J].时珍国医国药,2007,18(10):2381-2382. |
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| 作者姓名： | 霍金海 都晓伟 孙晖 陈雪英 |
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| 作者单位： | 黑龙江中医药大学药学院,黑龙江,哈尔滨,150040 |
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| 基金项目： | 黑龙江省杰出青年科学基金项目(No.JC200612) |
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| 摘 要： | 目的建立黑水缬草挥发油中乙酸龙脑酯的含量测定方法。方法采用气相色谱法,萘为内标物,DB-l7毛细管柱,载气为氦气,电子轰击(EI)离子源检测器。结果在该色谱条件下,乙酸龙脑酯在进样量0.109 6~1.753 6μg范围内呈良好线性关系,r=0.999 6;乙酸龙脑酯的加样回收率为101.33%,RSD=1.79%。结论该法能准确测定黑水缬草挥发油中乙酸龙脑酯的含量。
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| 关 键 词： | 气相色谱法 黑水缬草挥发油 乙酸龙脑酯 |
| 文章编号： | 1008-0805（2007）10-2381-02 |
| 收稿时间： | 2007-02-15 |
| 修稿时间： | 2007-05-15 |
Determination of Bornyl Acetate in Valeriana amurensis Volatile Oil by Gas Chromatography |
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| HUO Jin-hai,DU Xiao-wei,SUN Hui,CHEN Xue-ying.Determination of Bornyl Acetate in Valeriana amurensis Volatile Oil by Gas Chromatography[J].Lishizhen Medicine and Materia Medica Research,2007,18(10):2381-2382. |
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| Authors: | HUO Jin-hai DU Xiao-wei SUN Hui CHEN Xue-ying |
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| Institution: | Pharmaceutical College, Heilongjiang University of Chinese Medicine, Harbin 150040, China |
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| Abstract: | Objective To establish the method for determination of bornyl acetate in Valeriana amurenis volatile oil by Gas Chro- matography. Methods The GC system consisted of DB - 17capillary column, helium as the carrier gas and EI as the detector. Naphthalene was used as internal standard substance in the analysis method. Results The standard curve of bornyl acetate was linear over the range of 0. 109 6 - 1. 753 6 ixg,r = 0.999 6. The mean recovery of bornyl acetate was 101.33% ,RSD = 1.79%. Conclusion The method can accurately determine the content of bornyl acetate in Valeriana amureruis volatile oil. |
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| Keywords: | GC Valeriana amurensis volatile oil Bornyl acetate |
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