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气相色谱法测定蛹油中α-亚麻酸乙酯的含量
引用本文:李群,周淑平,张筱红. 气相色谱法测定蛹油中α-亚麻酸乙酯的含量[J]. 中国药品标准, 2002, 3(3): 47-48
作者姓名:李群  周淑平  张筱红
作者单位:1. 北京市药品检验所,北京,100035
2. 国家药典委员会,北京,100061
摘    要:
目的:用气相色谱内标法测定蛹油α-亚麻酸乙酯制剂中α-亚麻酸乙酯的含量。方法:采用气相色谱法,DEGS为固定相,涂布浓度为10%,载体为Chromosorb W AW DMCS80-100目的气相柱。结果:平均回收率为97.87%,RSD为1.52%。结论:该法操作简便、准确、重现性、稳定性好,可作为蛹油α-亚麻酸乙酯的含量测定方法。

关 键 词:蛹油α-亚麻酸乙酯 乙相色谱法 α-亚麻酸乙酯 含量测定

DETERMINATION OF ETHYI LINOLENATE IN BOMBYX MORI OIL ETHYL LINELENATE BY GAS CHROMATOGRAPHY
Li Qun,Zhou Shuping and Zhang Xiaohong. DETERMINATION OF ETHYI LINOLENATE IN BOMBYX MORI OIL ETHYL LINELENATE BY GAS CHROMATOGRAPHY[J]. , 2002, 3(3): 47-48
Authors:Li Qun  Zhou Shuping  Zhang Xiaohong
Affiliation:Li Qun Zhou Shuping Zhang Xiaohong(Beijing Municipal Institute for Drug Control 100035)(State Pharmacopoeia Commission of China 100061)
Abstract:
Purpose: The aim was to determine the ethyl linolenate in Bombyx mori oil ethyl linolenate by Gas Chromatography(GC).Methods:The method employed Gas Chromatography,Stationary Phose: Chrosorb W AW DMCS 80-100 mesh coated with 10% DEGS.Results:The recovery was 97.87% and the RSD was 1.52%.Conclusion:This method was convenient,accurate and steady,so it was suitable for assay of ethyl linolenate in Bombyx mori oil ethyl linolenate.
Keywords:Bombyx mori oil ethyl linolenate  Gas Chromatography  ethyl linolenate
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