| 黄芩中黄芩苷浸取工艺优化 |
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| 引用本文： | 周芳,池汝安,吴元欣,巨修炼,郭嘉,黄齐茂. 黄芩中黄芩苷浸取工艺优化[J]. 中药材, 2007, 30(3): 332-335 |
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| 作者姓名： | 周芳 池汝安 吴元欣 巨修炼 郭嘉 黄齐茂 |
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| 作者单位： | 武汉化工学院化工与制药学院,湖北省新型反应器与绿色化学工艺重点实验室,湖北武汉,430073 |
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| 摘 要： | 目的:优选黄芩中黄芩苷的浸取工艺。方法:采用正交设计试验,以黄芩苷浸取率为指标,对影响黄芩中黄芩苷浸取工艺的因素进行了考察,比较了乙醇回流法与水煎煮法、超声波法、半仿生法的黄芩苷浸取率。结果:在浸取温度为80℃,浸取时间为1 h,乙醇浓度为60%,搅拌速度为400 r/min时,黄芩苷的浸取率最高,达83.09%。同时,结果表明,乙醇回流法在黄芩苷的浸取中优于其它的方法。结论:醇提法浸取效率高,经济,浸取剂利于回收,适合工业化生产。
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| 关 键 词： | 黄芩 浸取 黄芩苷 |
| 文章编号： | 1001-4454(2007)03-0332-04 |
| 修稿时间： | 2006-09-04 |
The Optimum Condition on Baicalin Extraction from Scutellaria baicalensis |
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| ZHOU Fang,CHI Ru-an,WU Yuan-xin,JU Xiu-lian,GUO Jia,HUANG Qi-mao. The Optimum Condition on Baicalin Extraction from Scutellaria baicalensis[J]. Journal of Chinese medicinal materials, 2007, 30(3): 332-335 |
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| Authors: | ZHOU Fang CHI Ru-an WU Yuan-xin JU Xiu-lian GUO Jia HUANG Qi-mao |
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| Affiliation: | Hubei Key Lab of Novel Reactor & Green Chemical Technology, Wuhan Institute of Technology, Wuhan 430073, China. |
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| Abstract: | OBJECTIVE: To optimize the extraction process of baicalin from Scutellaria Baicalensis Georgi with ethanol. METHODS: The extraction process of baicalin from Scutellaria Baicalensis Georgi was optimized with the aid of orthogonal experiments. RESULTS: The optimal parameters were obtained as follows: extracting temperature, extracting time, ethanol concentration and mechanical stirring speed were 80 degrees C, 1 h, 60% and 400 r/min, respectively. The extracting rate of baicalin was 83.90%. CONCLUSION: Comparing ethanol circumfluence, boiling water, ultrasonic wave and semi-bionic on extracting baicalin from Scutellaria baicalensis Georgi, the ethanol circumfluence extraction is better than other technological conditions on extracting baicalin. |
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| Keywords: | Scutellaria baicalensis Extraction Baicalin |
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