| 大叶南五味子果实化学成分研究 |
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| 引用本文： | Wang HJ,Wu XL,Zhou TZ,Deng XM,Wang DC. 大叶南五味子果实化学成分研究[J]. 中药材, 2012, 35(3): 396-399 |
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| 作者姓名： | Wang HJ Wu XL Zhou TZ Deng XM Wang DC |
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| 作者单位： | 辽宁医学院;吉林大学;天津市宝坻区人民医院 |
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| 基金项目： | 国家自然科学基金(30800835);辽宁省教育厅项目(L2010256) |
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| 摘 要： | 目的:研究大叶南五味子果实的化学成分。方法:采用硅胶柱层析、Sephadex LH-20、HPLC等色谱技术进行分离纯化,NMR和EI-MS等波谱学方法进行结构鉴定,结果:从中分离得到9个化合物,分别鉴定为:4,5-二羟基-3-甲氧基二苯(Ⅰ)、eriobofuran(Ⅱ)、3β,16β-二羟基-12-烯-乌苏烷(Ⅲ)、2α,3β,6β,23-tetrahydroxy urs-12,18-dien-28-oic acid(Ⅳ)、2α,3β,23-trihydroxy urs-12-en-28-oic acid(Ⅴ)、芦丁(Ⅵ)、2-乙基己酸(Ⅶ)、2-月桂酸单甘油酯(Ⅷ)、单蓖麻油酸甘油酯(Ⅸ)。结论:以上9个化合物均为首次从南五味子属植物中分离得到。
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| 关 键 词： | 大叶南五味子 化学成分 |
Chemical constituents from the fruits of Kadsura marmorata |
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| Wang Hong-Jun,Wu Xin-Liang,Zhou Tie-Zhong,Deng Xu-Ming,Wang Da-Cheng. Chemical constituents from the fruits of Kadsura marmorata[J]. Journal of Chinese medicinal materials, 2012, 35(3): 396-399 |
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| Authors: | Wang Hong-Jun Wu Xin-Liang Zhou Tie-Zhong Deng Xu-Ming Wang Da-Cheng |
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| Affiliation: | Liaoning Medical University, Jinzhou 121001, China. wanghj0312@yahoo.com.cn |
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| Abstract: | Objective:To study the chemical constituents from the fruits of Kadsura marmorata.Methods:The chemical constituents were isolated and purified by chromatography on silica gel,Sephadex LH-20 column and HPLC. Results:9 compounds were isolated and identified as 4,5-dihydroxy-3-methoxybiphenyl(Ⅰ),eriobofuran(Ⅱ),3β,16β-dihydroxy urs-12-ene(Ⅲ),2α,3β,6β,23-tetrahydroxy urs-12,18-dien-28-oic acid(Ⅳ),2α,3β,23-trihydroxy urs-12-en-28-oic acid(Ⅴ),rutin(Ⅵ),2-ethylhexanoic acid(Ⅶ),2-monolaurin(Ⅷ),glyceryl monoricinoleate(Ⅸ) on the basis of NMR and EI-MS spectroscopic analysis.Conclusion:All these compounds are isolated from this genus for the first time. |
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| Keywords: | Kadsura marmorata (E.G.Henderson & A.Henderson)A.C.Smith Chemical constituents |
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