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GC-MS法分析山柰饮片挥发油的化学成分
引用本文:张桂芝.GC-MS法分析山柰饮片挥发油的化学成分[J].亚太传统医药,2007,3(7):56-59.
作者姓名:张桂芝
作者单位:徐州师范大学化学化工学院,江苏,徐州,221116
摘    要:目的:分析山柰饮片挥发油的化学成分。方法:水蒸气蒸馏法提取样品挥发油后,用气相色谱-质谱法分析,并用峰面积归一化法测定化学成分的相对含量。结果:从挥发油的69个色谱峰中共鉴定出54种化合物,占挥发油总成分的97.52%。主要成分依次为反式对甲氧基桂皮酸乙酯(33.84%),反式桂皮酸乙酯(28.30%),十五烷(14.85%),蓝桉醇(2.35%)。结论:山柰饮片挥发油的化学成分与文献相比有显著差异。

关 键 词:山柰  挥发油  气相色谱—质谱法  化学成分
文章编号:1673-2197(2007)07-056-04

Analysis of Constituents of Essential Oils in Rhizoma Kaempferiae by GC-MS
ZHANG Gui-zhi.Analysis of Constituents of Essential Oils in Rhizoma Kaempferiae by GC-MS[J].Asia-Pacific Traditional Medicine,2007,3(7):56-59.
Authors:ZHANG Gui-zhi
Abstract:Objective:To analyze Chemical Constituents of essential oils of Rhizoma Kaempferiae.Methods:Essential oils were extracted from samples by steam distillation,were determined by GC-MS,and with area normalization method.Results:54 components were identified from 69 chromatographic peaks of essential oils,which compose of 97.52% of the total essential oil.The main compounds of in essential oils were Ethyl-p-methoxycinnamate(32.08%),Ethyl-cinnamate(28.30%),Pentadecane(14.85%),Globulol(2.35%).Conclusion:Chemical Constituents of essential oils of Rhizoma Kaempferiae was signifcantly different than in references.
Keywords:Rhizoma Kaempferiae  Essential oils  C-C-MS  Chemical constituents
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