| 藏药八味獐牙菜丸的质量标准研究 |
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| 引用本文： | 逯雯洁,林鹏程. 藏药八味獐牙菜丸的质量标准研究[J]. 北方药学, 2014, 0(9): 2-4 |
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| 作者姓名： | 逯雯洁 林鹏程 |
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| 作者单位： | 青海省食品药品检验所 西宁 810003;青海民族大学 西宁 810007;青海民族大学 西宁 810007 |
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| 摘 要： | 目的：建立测定藏药八味獐牙菜丸中盐酸小檗碱含量的方法。方法：采用薄层色谱法和高效液相色谱法。结果：建立了八味獐牙菜丸中兔耳草和小檗皮的薄层色谱鉴别方法,并采用HPLC测定了该藏药制剂中小檗皮的有效成分盐酸小檗碱的含量,其回归方程为：y=4629102.46x-136034.70,r=0.9995,盐酸小檗碱的平均回收率为97.30%,RSD=1.57%（n=6）。结论：该方法测定快速、重现性好,可用于八味獐牙菜丸的质量控制。
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| 关 键 词： | 薄层色谱法 高效液相色谱法 盐酸小檗碱 八味獐牙菜丸 |
Quality Control of Bawei Zhangyacai Pill |
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| Affiliation: | Lu Wenjie,Ling Pengcheng (1.Qinghai Provincial Institute of Food and Drug Control, Qinghai Xining 810003, China;2.Qinghai University For Nationalities, Xining, Qinghai, 810007, China) |
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| Abstract: | Objietive：To establish a TLC identification and an HPLC quantitative determination methods for Bawei Zhangyacai Pills. Methods： TLC arid HPLC were used.Results：The TLC method could identify Lagotis glauca Gaertn and Berberis kansuensis Schneid , and HPLC method could quantitive determine Berberine Hydrochloride quantity in Bawei Zhangyacai Pills. The regression equation of standard curve was y=4629102.46x -136034.70,r =0.9995,the mean reeovery was 97.30% with RSD ofl.57% for the HPLC method. Conclusions：This method is simple, rapid and reliable with good reprodueibility, and can be used to control the quality of Bawei Zhangyaeai Pills. |
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| Keywords: | TLC HPLC Berberine Hydrochloride Bawei Zhangyacai Pill |
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