| 补肾温肺合剂的质量控制 |
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| 引用本文： | 胡雪来,刘水平. 补肾温肺合剂的质量控制[J]. 中国药师, 2009, 12(10): 1404-1405 |
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| 作者姓名： | 胡雪来 刘水平 |
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| 作者单位： | 1. 湖南中医药高等专科学校附属第一医院,湖南株洲,412000
2. 株洲市药品检验所 |
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| 摘 要： | 目的：建立补肾温肺合剂的质量控制方法。方法：用薄层色谱法对补肾温肺合剂中黄芪进行定性鉴别；采用高效液相色谱法测定补肾温肺合刑中淫羊藿苷的含量。结果：薄层色谱中斑点清晰，易于识别；淫羊藿苷线性范围为0．20—4．08p,g（r=0．9998），平均回收率为98．88％，RSD=1．27％。结论：本方法简便，灵敏度高，可有效地控制补肾温肺舍剂的质量。
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| 关 键 词： | 补肾温肺合剂 薄层色谱法 高效液相色谱法 淫羊藿苷 |
Quality Control of Bushen Wenfei Mixture |
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| Affiliation: | Hu Xuelai,Liu Shuiping (1.First Affiliated Hospital of Hunan Traditional Chinese Medical College, Hunan Zhuzhou 412000, China;2.Zhuzhou Institute for Drug Control) |
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| Abstract: | Objective： To establish a method for quality control of bushen wenfei mixture. Method： The Radix Astragali was identiffed by TLC ;The content of Icariine was measured by HPLC. Result： The spots in TLC were clear and well distinguished. The method was linear within a range of 0.20 - 4.08 μg for the berberine hydrochloride （ r = 0.999 8 ）, The average recovery was 98.88%, and within-day RSD was 1.27%. Condttsion： The method is simple, sensitive and accurate. It can be used to control the quality of bushen wenfei mixture. |
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| Keywords: | Bushen wenfei mixture TLC RP-HPLC Icariine |
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