|
|||||
|
|
| 大孔吸附树脂用于小檗碱的富集与定量分析 | |
| 引用本文： | 罗集鹏,马红文,许敏青,陈新. 大孔吸附树脂用于小檗碱的富集与定量分析[J]. 中药材, 2000, 23(7): 413-415 |
| 作者姓名： | 罗集鹏 马红文 许敏青 陈新 |
| 作者单位： | 1. 广东药学院,510224 2. 广东省茂名市药品检验所,525011 |
| 摘 要： | 采用大孔吸附树脂对黄连药材及其制剂中小檗碱进行了订，并用ＨＰＬＣ法进行定量分析。 |
| 关 键 词： | 黄连 小檗碱 大孔吸附树脂 HPLC 定量分析 |
| 修稿时间： | 1999-03-18 |
HPLC Quantitative Analysis of Berberine Absorpted with Macroporous Resin in Rhizoma Coptidis and Its Preparation Zuo Jin Wan |
|
| Luo Jipeng,Ma Hongwen,Xu Minqin. HPLC Quantitative Analysis of Berberine Absorpted with Macroporous Resin in Rhizoma Coptidis and Its Preparation Zuo Jin Wan[J]. Journal of Chinese medicinal materials, 2000, 23(7): 413-415 | |
| Authors: | Luo Jipeng Ma Hongwen Xu Minqin |
| Affiliation: | Guangdong College of Pharmacy, Guangzhou 510224. |
| Abstract: | Absorptive ability and elution program of macroporous resin to the berberine in the Rllizoma Coptidis and its preparation Zuo Jin Wan (containing Rhizoma Coptidia and Fructus Evodiae) were explored. The extract of 70% MeOH of samples we disolved in water, then alkalized to pH 12 with ammonia solution. The berberine was absorpted by the macroporous resin, the washed off water soluble impurity with alkalescent water, and eluted with 50% MeOH containing 0.5% H2SQ4. The results of quantitative analysis of the berberine by HPLC were satisfied. |
| Keywords: | Rhizoma Coptidis and its preparation Zuo Jin Wan Berberine Macroporous resin HPLC Quantitative analysis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |