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甘露消毒颗粒中挥发油的指纹图谱建立
引用本文:刘文龙,贺福元,张喜利. 甘露消毒颗粒中挥发油的指纹图谱建立[J]. 中成药, 2005, 27(8): 869-872
作者姓名:刘文龙  贺福元  张喜利
作者单位:1. 湖南中医学院药学院,湖南,长沙,410007
2. 湖南九芝堂制药有限公司,湖南,长沙,410007
摘    要:
目的:对甘露消毒颗粒(飞滑石、绵茵陈、淡黄芩等)中的挥发油进行研究,建立其挥发油的指纹图谱.方法:用毛细管气相色谱法.结果:所建立的挥发油指纹图谱,有色谱峰约56个,其中特征峰17个(占总面积的86.97%),其共有峰的相对保留时间RSD的平均值为0.33%,相对峰面积RSD的平均值为2.76%.结论:用此法可以建立有效的指纹图谱,给甘露消毒丹的质量控制提供了方法.

关 键 词:甘露消毒丹  挥发油  指纹图谱  毛细管气相色谱
文章编号:1001-1528(2005)08-0869-04
收稿时间:2004-07-10
修稿时间:2004-07-10

Fingerprint of volatile in Ganlu Xiaodu Granules
LIU Wen-long,HE Fu-yuan,ZHANG Xi-li. Fingerprint of volatile in Ganlu Xiaodu Granules[J]. Chinese Traditional Patent Medicine, 2005, 27(8): 869-872
Authors:LIU Wen-long  HE Fu-yuan  ZHANG Xi-li
Abstract:
AIM: To study the volatile oil of GanluXiaodu Granules GLXD (Talcum, Herba Artemisiae Scopariae, Radix Scutellariae etc.) and establish it's fingerprint. METHODS: By capillary gas chromatography. RESULTS: The fingerprints of volatile oil in Ganlu Xiaodu Granules were composed of 56 peaks, among which there were 17 characteristic peaks, having 86.97% of total area of the whole fingerprints peaks. The average RSD of retention time of characteristic peaks was 0.33%, that of peak-area was 2.76%. CONCLUSION: The fingerprints of volatile in Ganlu Xiaodu Granules can be used to control the quality.
Keywords:Ganlu Xiaodu Granules  volatile  fingerprints  capillary gas chromatography  
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