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| 清解利感合剂质量标准研究 | |
| 引用本文： | 李甲英,李安华. 清解利感合剂质量标准研究[J]. 儿科药学, 2014, 0(8): 30-33 |
| 作者姓名： | 李甲英 李安华 |
| 作者单位： | 云南中医学院,云南昆明650500 |
| 基金项目： | 云南省科技厅项目,项目编号：2008IF014 |
| 摘 要： | 目的：建立清解利感合剂的质量标准,完善质量控制体系。方法：采用TLC法对清解利感合剂方中金银花、连翘、防风、射干、牛蒡子进行定性分析；HPLC法对其有效成分连翘苷进行含量测定。结果：TLC法可准确地对金银花、连翘、防风、射干、牛蒡子进行定性鉴别；连翘苷在0.1～1.0 mg/mL范围内线性关系良好（r=0.9999）；平均回收率为99.08%,RSD=2.42%（n=6）。结论：本方法简便、快速、重现性好,所建标准可用于清解利感合剂的质量控制。 |
| 关 键 词： | 清解利感合剂 质量标准 薄层色谱法 高效液相色谱法 |
Quality Standard of Qingjieligan Mixture |
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| Li Jiaying,Li Anhua. Quality Standard of Qingjieligan Mixture[J]. Journal of Pediatric Pharmacy, 2014, 0(8): 30-33 | |
| Authors: | Li Jiaying Li Anhua |
| Affiliation: | (Yunnan University of Traditional Chinese Medicine, Yunnan Kunming 650500, China) |
| Abstract: | Objective： To establish quality standard of Qingjieligan Mixture. Methods： The qualitative analysis of Flos lonicerace,Forsythin,Saposhnikovia divaricata,Rhizoma Belamcandae and Arctium Lappa L. was performed using TLC. The content of Forsythin in the Qingjieligan Mixture was determined by HPLC. Results： Flos lonicerace,Forsythin,Saposhnikovia divaricata,Rhizoma Belamcandae and Arctium Lappa L. could be accurately identified by TLC. Forsythin showed good linearity within the range of 0. 1 ～ 1. 0 mg /mL（r = 0. 9999）,and its average recovery was 99. 08% with RSD at 2. 42%（ n = 6）. Conclusions： The method is simple,rapid and reproducible,and can be used for the quality control of Qingjieligan Mixture. |
| Keywords: | Qingjieligan Mixture Quality standard TLC HPLC |
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