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舒阴洗液质量标准研究
引用本文:刘光斌,任洁.舒阴洗液质量标准研究[J].中医药学刊,2010(11):2438-2439.
作者姓名:刘光斌  任洁
作者单位:甘肃省酒钢医院,甘肃嘉峪关735100
摘    要:目的:研究舒阴洗液的质量标准。方法:采用薄层色谱法鉴别苦参、白鲜皮、蛇床子;采用高效液相色谱法测定苦参中有效成分苦参碱的含量。结果:鉴别方法专属性强,重现性好,空白无干扰;苦参碱在3.9~117.0μg之间呈良好的线性关系(r=0.9999),平均回收率为101.69%,RSD=1.84%(n=9)。结论:本研究中建立的定性定量方法操作简便,专属性强,准确可靠,可以有效控制舒阴洗液质量。

关 键 词:舒阴洗液  薄层色谱  高效液相色谱  苦参碱

Studies on Quality Standards for Shuyin Lotion
LIU Guang-bin,REN Jie.Studies on Quality Standards for Shuyin Lotion[J].Study Journal of Traditional Chinese Medicine,2010(11):2438-2439.
Authors:LIU Guang-bin  REN Jie
Institution:(Jiugang Hospital of Gansu, Jiayuguan 735100, Gansu, China)
Abstract:Objective:To establish the quality standard of Shuyin Lotion.Methods:Sophora Flavescens Ait,Cortex Dict-amni,Fructus Cnidii in Shuyin Lotion were identified by TLC,and content of matrine was determined by HPLC.Results:The method for identification had good specificity and repeatability.There was no interference in blank control.The cali-bration curve of matrine was linear in range of 3.9 ~ 117.0 μg(r = 0.99999).The average recovery was 101.69% with RSD of 1.84%(n = 9).Conclusion:The qualitative and quantitative method is simple,specific,accurate and reliable.It can be used to effectively control the quality of Shuyin Lotion.
Keywords:Shuyin Lotion  TCL  HPLC  matrine
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