|
|||||
|
|
| 复方板蓝根颗粒中靛玉红的含量测定 | |
| 引用本文： | 杜萍,刘少娟,刘永俊. 复方板蓝根颗粒中靛玉红的含量测定[J]. 齐鲁药事, 2010, 29(6): 338-339 |
| 作者姓名： | 杜萍 刘少娟 刘永俊 |
| 作者单位： | 1. 烟台市职业学院,山东,烟台264670 2. 烟台市药品检验所,山东,烟台264000 3. 烟台天正药业有限公司,山东,烟台,264000 |
| 摘 要： | 目的测定复方板蓝根颗粒中靛玉红的含量。方法高效液相色谱法。色谱柱为Hypersil BDS C18(5μm,4.6mm×250mm),柱温:35℃;甲醇-水(66∶34)为流动相;流速1mL·min-1;检测波长为292nm。结果靛玉红在进样量为0.0015～0.0375μg范围内与峰面积呈良好的线性关系,平均回收率为101.06%,RSD值为0.96%。结论该法可用于复方板蓝根颗粒中靛玉红的含量测定。 |
| 关 键 词： | 复方板蓝根颗粒 靛玉红 高效液相色谱法 |
Determination of indirubin in Fufang Banlangen Granules by HPLC |
|
| DU Ping,LIU Shao-juan,LIU Yong-jun. Determination of indirubin in Fufang Banlangen Granules by HPLC[J]. qilu pharmaceutical affairs, 2010, 29(6): 338-339 | |
| Authors: | DU Ping LIU Shao-juan LIU Yong-jun |
| Affiliation: | (Yantai Vocational College, Yantai 264670;1. Yantai Institute for Drug Control, Yantai 264000 2. Yantai Tianzheng Pharmaceutical Limited Company, Yantai 264000) |
| Abstract: | OBJECTIVE To determine indirubin in Fufang Banlangen Granules. METHODS The HPLC analysis was carried out on Hypersil BDS C18 （5μm, 4.6mm × 250mm）, the mixture of methanol-water （66 ： 34）was used as the mobile phase,the flow rate was 1 mL ·min^-1, the detection wavelength was 292nm. RESULTS The linear range of indirubin was 0. 0015-0. 0375μg. The average recovery of this method was 101.06% and the RSD was 0. 96%. CONCLUSION The method can be applied in determanition of indirubin in Fufang Banlangen Granules. |
| Keywords: | Fufang Banlangen Granules indirubin HPLC |
| 本文献已被 维普 万方数据 等数据库收录！ | |