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| HPLC法测定蒙药玉簪清咽十五味散中栀子苷的含量 | |
| 引用本文： | 包明兰,付长友,淑艳. HPLC法测定蒙药玉簪清咽十五味散中栀子苷的含量[J]. 辽宁中医杂志, 2008, 35(5): 753-754 |
| 作者姓名： | 包明兰 付长友 淑艳 |
| 作者单位： | 内蒙古民族大学蒙医药学院,内蒙古,通辽028000;兴安盟科右中旗公安局,内蒙古,兴安盟029400 |
| 摘 要： | 目的:建立蒙药玉簪清咽十五味散的质量标准。方法:用高效液相色谱法对处方中栀子有效成分栀子苷进行定量分析。采用VP-ODS(150L×4.6)柱,流动相:乙腈-0.1%磷酸水溶液(15:85V/V),检测波长:238nm,流速:0.5mL/min。结果:栀子苷进样量在30～150μg范围内与峰面积线性关系良好(r=0.9998)。平均加样回收率为97.6%(RSD=0.51%)。结论:本试验方法即先进又简便、结果准确可靠为该制剂的质量标准提供可靠依据。 |
| 关 键 词： | 玉簪清咽十五味散 HPLC 栀子苷 含量测定 |
| 文章编号： | 1000-1719(2008)05-0753-02 |
| 修稿时间： | 2007-12-04 |
Determination of Geniposide in Yuzan Qingyan Shiwuwei by HPLC |
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| BAO Ming-lan,FU Chang-you,SHU Yan. Determination of Geniposide in Yuzan Qingyan Shiwuwei by HPLC[J]. Liaoning Journal of Traditional Chinese Medicine, 2008, 35(5): 753-754 | |
| Authors: | BAO Ming-lan FU Chang-you SHU Yan |
| Affiliation: | BAO Ming-lan1,FU Chang-you2,SHU Yan1 |
| Abstract: | Objectives:To establish the quality standard for Yuzan Qingyan Shiwuwei Powder.Methods:The chromatographic conditions were listed below:VP-ODS(150L×4.6) conlumn,UV detector at 238nm of wavelength,a mobilphase of CH3CN-0.1%H3PO4(15∶85 V/V),and 0.5mL·min-1 of flow rate.Results:The calibration curves were linear for geniposide with in 30～150μg(r=0.9998).The recoveries were 97.6%(RSD=0.51%) for geniposide.Conclusion:This mehtod is simple and the separate result is satisfactory. |
| Keywords: | HPLC |
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