| 广西甜茶化学成分的研究 |
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| 引用本文： | 王剑霞,吕华冲. 广西甜茶化学成分的研究[J]. 中药材, 2007, 30(7): 800-802 |
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| 作者姓名： | 王剑霞 吕华冲 |
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| 作者单位： | 广东药学院天然药物化学教研究,广东广州,510006 |
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| 基金项目： | 红外、核磁共振、质谱均由中山大学分析测试中心测定,特此致谢! |
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| 摘 要： | 目的:研究广西甜茶(Rubus suavissimus S.Lee)叶中的活性成分。方法:利用反复硅胶柱层析的方法对广西甜茶进行分离和纯化,通过IR、MS、NMR等光谱技术和化学方法鉴定化合物的结构。结果:从广西甜茶叶中分离得到2个对映-贝壳杉烯型二萜类化合物,经鉴定化合物Ⅰ为对映-13-羟基-贝壳杉-16-烯-19-羧酸(ent-13-hydrox-y-kauran-16-en-19-oic acid),化合物Ⅱ为对映-贝壳杉-16-烯-19-酸-13-O-β-D-葡萄糖苷(ent-kauran-16-en-19-oic-13-O-β-D-glucoside)。结论:化合物Ⅱ为首次从该植物中分得。
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| 关 键 词： | 广西甜茶 对映-贝壳杉烯 二萜 二萜苷 |
| 文章编号： | 1001-4454（2007）07-0800-03 |
| 修稿时间： | 2006-12-25 |
Studies on the Chemical Constituents of Rubus suavissimus S. Lee |
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| WANG Jian-xia,L Hua-chong. Studies on the Chemical Constituents of Rubus suavissimus S. Lee[J]. Journal of Chinese medicinal materials, 2007, 30(7): 800-802 |
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| Authors: | WANG Jian-xia L Hua-chong |
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| Affiliation: | Department of Phytochemistry, Guangdong College of Pharmacy, Guangzhou 510006, China |
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| Abstract: | OBJECTIVE: To study the bioactive constituents from leaves of Rubus suavissimus S. Lee. METHODS: Column chromatography with silic gel was employed to isolate and purify the constituents. Their structures were elucidated by means of IR, MS, NMR and chemical methods respectively. RESULTS: Two consituents were obtained, which were elucidated as ent-13-hydroxy-kauran-16-en-19-oic acid (I), ent-kaura-16-en-19-oic-13-O-beta-D-glucoside (II), respectively. CONCLUSION: Compound II was seperated from Rubus suavissimus S. Lee for the first time. |
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| Keywords: | Rubus suavissimus S.Lee Ent-kaurene Diterpenoid Diterpene-glucoside |
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