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| 健肾壮腰力质量标准的研究 | |
| 引用本文： | 蒋秋桃,孙辉,文庆. 健肾壮腰力质量标准的研究[J]. 海峡药学, 2011, 23(9): 59-61 |
| 作者姓名： | 蒋秋桃 孙辉 文庆 |
| 作者单位： | 湖南省药品检验所,长沙,410001 |
| 基金项目： | 国家药典委员会国家药品标准提高行动计划项目 |
| 摘 要： | 目的 建立健肾壮腰丸质量标准.方法 采用TLC对女贞子、金樱子、制何首乌进行鉴别;用HPLC法测定2,3,5,4'-四羟基二苯乙烯-2-O-β-D-葡萄糖苷的含量,色谱柱为Shimadzu VP-ODS(150mm×4.6mm×5μm).流动相为乙腈-0.3%磷酸溶液(15:85),流速为1.OmL·min-1,检测波... |
| 关 键 词： | 健肾壮腰丸 质量标准 薄层色谱法 高效液相色谱法 |
Study on quality standard for Jianshen Zhuangyao Pills |
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| JIANG Qiu-tao,SUN Hui,WEN Qing. Study on quality standard for Jianshen Zhuangyao Pills[J]. Strait Pharmaceutical Journal, 2011, 23(9): 59-61 | |
| Authors: | JIANG Qiu-tao SUN Hui WEN Qing |
| Affiliation: | JIANG Qiu-tao,SUN Hui,WEN Qing(Institute for Drug of Hunan Province,Changsha 410001,China) |
| Abstract: | OBJECTIVE To establish quality standard for Jianshen Zhuangyao Pills.METHODS Ligustri Lucidi Fructus,Rosae Laevigatate Fructus and Polygoni Multiflori Radix Praeparata in this medicine were identified by TLC;Shimadzu VP-ODS(150mm×4.6mm×5μm)was eluted with mobile phase consisted of acetonitrile-0.3%aqueous phosphoric aicd(15∶85)at the column temperature 30℃.The flow rate was 1.0mL·min-1 and detective wavelength was 320nm.RESULTS The TLC spots developed were quite clear.The linear range of 2,3,5,4/-tetrahydroxystilbene-2-O-β-D-gulcoside was within 0.02522～5.044μg(r=0.9999),the average recovery(n=9)was 100.6%(RSD was 2.8%).CONCLUSION The method is simple,reliable,accruate and can be applied to quality control of Jianshen Zhuangyao Wan. |
| Keywords: | Jianshen Zhuangyao Pills Quality srandard TLC HPLC |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |