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| 玻璃输液瓶中锑浸出量的原子荧光光谱法测定 | |
| 引用本文： | 周红娇. 玻璃输液瓶中锑浸出量的原子荧光光谱法测定[J]. 海峡药学, 2011, 23(4): 66-68 |
| 作者姓名： | 周红娇 |
| 作者单位： | 云南省医疗器械检验所,昆明,650034 |
| 摘 要： | 目的建立氢化物发生-原子荧光光谱法HG-AFS测定药包材中玻璃输液瓶的锑浸出量方法。方法样品液直接用原子荧光光谱法测定,并对HG-AFS工作参数及条件进行优化和选择。结果标准曲线线性良好,相关系数r=0.9996,检出限0.087μg.L-1,回收率97.53%,RSD为4.92%。结论方法简便、快速准确、灵敏度高。 |
| 关 键 词： | 氢化物发生-原子荧光光谱法 药包材 玻璃输液瓶 锑浸出量 |
Determination of antimony releases from glass infusion bottles of drug packaging materials by hydride generation-atomic fluorescence spectrometry |
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| ZHOU Hong-jiao. Determination of antimony releases from glass infusion bottles of drug packaging materials by hydride generation-atomic fluorescence spectrometry[J]. Strait Pharmaceutical Journal, 2011, 23(4): 66-68 | |
| Authors: | ZHOU Hong-jiao |
| Affiliation: | ZHOU Hong-jiao(Yunnan Province Institute of Testing on Medical Appliance,Kunming 650034,China) |
| Abstract: | OBJECTIVE To establish a method for determination of antimony release from Glass Infusion bottles of drug packaging materials by hydride generation-atomic fluorescence spectrometer(HG-AFS).METHODS Sample solutions were directly determined by HG-AFS.Operation parameters of HG-AFS and condition were optimized and selected.RESULTS A good linearity was obtained(r=0.9996).The detection limit was 0.087μg·L-1.The recovery was 97.53%.RSD was 4.92%.CONCLUSION The method was simple and fast with high sensitivity. |
| Keywords: | HG-AFS Drug packaging materials Glass Infusion bottles Release of antimony. |
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