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| 脑脉利颗粒中芍药苷，益母草碱，黄芪甲苷及盐酸水苏碱含量测定 | |
| 引用本文： | 苏梅,韩承业. 脑脉利颗粒中芍药苷，益母草碱，黄芪甲苷及盐酸水苏碱含量测定[J]. 药学与临床研究, 2015, 23(4) |
| 作者姓名： | 苏梅 韩承业 |
| 作者单位： | 江苏柯菲平医药股份有限公司,江苏柯菲平医药股份有限公司 |
| 摘 要： | 目的：建立脑脉利颗粒中芍药苷，益母草碱，黄芪甲苷及盐酸水苏碱的含量测定方法。方法：采用甲醇、酸水等不同的溶剂提取，并采用高效液相色谱法，液质联用法等灵敏、专属的色谱方法进行含量测定。结果：每10g脑脉利颗粒中含有芍药苷 42.41 mg，益母草碱 1.73mg，黄芪甲苷 0.10 mg，盐酸水苏碱 37.98mg。结论：制剂中其他组分与所测定的各组分分离良好，不干扰测定，可用于脑脉利颗粒中芍药苷，益母草碱，黄芪甲苷及盐酸水苏碱的含量测定。 |
| 关 键 词： | 脑脉利颗粒；芍药苷；益母草碱；黄芪甲苷；盐酸水苏碱 |
| 收稿时间： | 2014-12-29 |
| 修稿时间： | 2014-12-29 |
Determination of the Peoniflorin, Leonurine, Astragaloside, and Stachydrine hydrochloride in the NaoMaiLi particles |
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| sumei and hanchengye. Determination of the Peoniflorin, Leonurine, Astragaloside, and Stachydrine hydrochloride in the NaoMaiLi particles[J]. Pharmacertical and Clinical Research, 2015, 23(4) | |
| Authors: | sumei and hanchengye |
| Abstract: | Objective: To develop a method for determining contents of Peoniflorin, Leonurine, Astragaloside, and Stachydrine hydrochloride in NaoMaiLi particles. Method: To determine contents using methanol or acid extraction following high performance liquid chromatography or liquid chromatography-mass spectrometry. Results: Per 10g NaoMaiLi particles contain 42.41mg of Peoniflorin, 1.73mg of Leonurine, 0.10mg of Astragaloside, and 37.98mg of Stachydrine hydrochloride. Conclusion: The method is selective for determination of Peoniflorin, Leonurine, Astragaloside, and Stachydrine hydrochloride in NaoMaiLi particles. |
| Keywords: | NaoMaiLi Particles Peoniflorin Leonurine Astragaloside Stachydrine hydrochloride |
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