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夜合花挥发油化学成分的GC-MS分析
引用本文:朱小勇,邵敏敏,张宏建,卢汝梅.夜合花挥发油化学成分的GC-MS分析[J].中国实验方剂学杂志,2011,17(8):125-127.
作者姓名:朱小勇  邵敏敏  张宏建  卢汝梅
作者单位:广西中医学院,南宁,530001
摘    要:目的:研究夜合花挥发油的化学成分。方法:利用水蒸气蒸馏法及超临界CO2萃取法提取桂产夜合花挥发油,用GC-MS联用技术对其化学成分进行分离鉴定,用面积归一化法确定各成分的相对含量。结果:水蒸气蒸馏法提取的挥发油鉴定56个化合物,占挥发油总量的87.46%,超临界CO2萃取法提取的挥发油鉴定25个化合物,占总量的95.86%。结论:桂产夜合花挥发油主要成分是α-蒎烯、橙花叔醇、石竹烯、吉玛烯D、双环吉玛烯,与文献报道其他产地的夜合花挥发油成分有明显差异。

关 键 词:夜合花  挥发油  CO2超临界萃取  水蒸气蒸馏  气相色谱-质谱联用
收稿时间:2010/12/28 0:00:00

Analysis of Chemical Constituents of Essential Oils from Magnolia coco by GC-MS
ZHU Xiao-yong,SHAO Min-min,ZHANG Hong-jian and LU Ru-mei.Analysis of Chemical Constituents of Essential Oils from Magnolia coco by GC-MS[J].China Journal of Experimental Traditional Medical Formulae,2011,17(8):125-127.
Authors:ZHU Xiao-yong  SHAO Min-min  ZHANG Hong-jian and LU Ru-mei
Institution:Guangxi Traditional Chinese Medical University, Nanning 530001, China;Guangxi Traditional Chinese Medical University, Nanning 530001, China;Guangxi Traditional Chinese Medical University, Nanning 530001, China;Guangxi Traditional Chinese Medical University, Nanning 530001, China
Abstract:Objective:To study the chemical constituents of the essential oils from Magnolia coco.Method:The essential oils were extracted by steam distillation(SD) and supercritical carbon dioxide extraction(SFE),and then the constituents were separated and identified by GC-MS.Result:Fifty six compounds were isolated and identified by SD that composed about 87.46% of the total essential oils;and 25 compounds were isolated and identified by SFE that composed about 95.86% of the total essential oils.Conclusion:The princ...
Keywords:Magnolia coco  essential oils  steam distillation  supercritical carbon dioxide extraction  GC-MS
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