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The shelf-life of 10% sodium phenobarbital injection(containing propylene glycol 60%) has been predicted by accelerated stability test with the classical isothermal method (at 100, 90, 80 and 70℃). The data was treated with regressive calculation, and the shelf-life calculated with three different methods (regressive calculation, average activation energy calculation and graphical plotting).The values obtained from these three methods were approximately equal, and also coincided with the value obtained from samples reserved for observation at room temperature. The shelf-life was 1.05 years at 25℃, and 2.03 years at 20℃. 相似文献
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A major degradated product was obtained from sodium phenobarbital injection stored at room temperature or heated at 100℃ for a long time. It was identified by means of melting point, optical rotation, UV and IR spectrum, elemental analysis and paper chromatography to be dl-pheneturide irrespective of the source of sample.A search in the literature showed that this degradated product is a potent anticonvulsant. 相似文献
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