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221.
A Ferencz M Bacsó 《Clinica chimica acta; international journal of clinical chemistry》1983,135(1):103-106
A reliable high-performance liquid Chromatographic method is presented for the determination of the urinary free catecholamines noradrenaline, adrenaline and dopamine. Urine is purified on a column of immobilized boric acid. Catecholamines are separated by ion-pair reversed phase high-performance liquid chromatography and detected electrochemically.The method is suited for routine analysis. It allows the determination of urinary free catecholamines in concentrations as low as 1 μg/l for noradrenaline and adrenaline and 5 μg/l for dopamine. A single analysis can be completed within 1 h. Routine analyses can be carried out in a series of 40 samples within 2 days. The within-assay and between-assay coefficients of variation of the analyses in urine were both 2.9% for noradrenaline, both 5.0% for adrenaline, and 1.9 and 2.1% for dopamine.The Chromatographic properties of the immobilized boric acid were investigated. In particular, the elution pattern of a series of catecholamine metabolites and analogues was determined. Under the conditions used, only basic compounds containing both a vicinal hydroxyl configuration and a primary or secondary amino group adsorb and elute together with the free catecholamines. 相似文献
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360°滚转复位法治疗良性阵发性位置性眩晕 总被引:3,自引:1,他引:2
目的明确在后半规管平面360°旋转患者对治疗典型的后半规管良性阵发性位置性眩晕是否有效。方法回顾分析了46例后半规管良性阵发性位置性眩晕患者,其中25例采用三维滚轮360°滚转复位法进行复位治疗,21例采用Epley手法复位治疗,对其疗效进行比较。结果采用三维滚轮360。滚转复位法治疗的患者中第一次治疗后有23例患者(92%)治愈,2例患者经过第二次治疗治愈;采用Epley手法复位的患者中第一次治疗后有19例患者(91.5%)治愈,2例患者经过第二次治疗治愈。应用X^2检验(α=0.05,X^2=0.1173,P=0.7319)二者的差异没有统计学意义。结论三维滚轮360°滚转复位法能有效的治疗后半规管良性阵发性位置性眩晕,其成功率及效果与Epley法一致,且操作简便、舒适度优于传统方法。 相似文献
224.
目的 了解烟台市17类2717份食品中铅的污染状况。方法 采用随机采样的方法采集烟台市售17类2717份食品,依据国标规定的标准操作程序进行检测。结果 铅总体合格率为99.30%(2698/2717)。谷物及其制品、乳及乳制品、水产品及其制品和蔬菜及其制品的铅超标率分别为4.31%(10/232)、1.78%(4/225)、0.86%(3/348)和0.34%(2/594)。茶叶、调味品和藻类铅含量较高,均值分别为0.38mg/kg、0.30mg/kg、0.27mg/kg;焙烤食品、饮料铅含量较低,均未检出。不同食品亚类间比较,海洋软体动物、动物肝肾、大米、水生类蔬菜、核果类水果和乳粉铅含量较高,均值分别为0.15mg/kg、0.13mg/kg、0.11mg/kg、0.05mg/kg、0.04mg/kg、1.44×10-2mg/kg和0.04mg/kg。不同年度铅检出率基本呈现下降趋势,2013-2017年铅检出率分别为77.05%、73.81%、58.01%、34.97%和29.25%。本地、外地与产地不详样品超标率差异有统计学意义(〖XC五号.EPS;P〗=8.820,P=0.012);烟台市环渤海区、环黄海区、非沿海区、烟台市不详4个区域样品超标率无统计学意义(〖XC五号.EPS;P〗=7.120,P=0.068) 。结论 烟台市17类食品中铅污染状况较轻,但仍存在一定程度的残留污染。 相似文献
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Akihiko Hiyama MD PhD Taku Ukai MD PhD Shota Ogasawara MD Tatsumi Tanaka MD Masahiko Watanabe MD PhD 《Orthopaedic Surgery》2023,15(5):1405-1413
Objective
Fluoroscopy is often used in the surgery of unstable pelvic ring fractures, and improved safety in implant placement is an issue. An anterior subcutaneous pelvic fixator (INFIX) combined with a percutaneous screw has been reported to be a minimally invasive and effective surgical technique for unstable pelvic ring injuries. However, although percutaneous screw fixation is minimally invasive, its indications for fracture fixation and fractures with large fragment displacements in the vertical plane remain controversial. Therefore, this technical note aims to describe a new technique for unstable pelvic ring fractures.Methods
We describe a 360° fusion of the pelvic ring to treat unstable pelvic ring fractures, including vertical shear pelvic ring fractures, using an intraoperative CT navigation system. Seven patients were treated with 360° fusion for type C pelvic ring fractures. In surgery, after reducing the fracture with external fixation, intraoperative CT navigation is used to perform a 360° fusion with INFIX and minimally invasive surgical spinopelvic fixation (MIS-SPF). We will introduce a typical case and explain the procedure.Results
A 360° fixation was performed, and no perioperative complications were noted. The mean blood loss was 253.2 ± 141.0 mL, and the mean operative time was 224.3 ± 67.4 min. In a typical case, bone union was obtained 1 year after surgery, and we removed all implants.Conclusions
MIS-SPF has a strong fixation force and helps reduce fractures' horizontal and vertical planes. In addition, 360° fusion with intraoperative CT navigation may help treat unstable pelvic ring fractures. 相似文献228.