薄层扫描法测定跌打七厘片中血竭素的含量

目的 采用薄层扫描法测定跌打七厘片中血竭素的含量。方法 样品经适当提取、净化后点于硅胶G薄层板上，氯仿－甲醇（19：1）为展开剂，双波长反射法锯齿扫描，检测波长为λs＝480nm，λR＝560nm。结果 本法线性关系良好，平均加样回收率为96．2％，RSD值为2．4％。测得跌打七厘片中血竭素的含量约为0．038％。结论 本方法操作简单，准确，可用于跌打七厘片的质量控制。     

乳腺清胶囊薄层色谱鉴别研究

目的：研究乳腺清胶囊的质量控制方法。方法：采用薄层色谱法对乳腺清胶囊中青皮、重楼、香附、当归进行定性鉴别。结果：4项薄层色谱鉴别均具专属性。结论：方法可靠，可用于乳腺清胶囊的质量控制。     

芎术胶囊质量标准研究

目的：研究中药制剂芎术胶囊的质控标准。方法：用显微和薄层色谱鉴别控制质量。结果：方法简便，专属性强，重现性好。结论：通过对处方中主药用显微和薄层色谱鉴别，可有效的控制芎术胶囊质量。     

通脉灵胶囊薄层色谱鉴别研究

目的：完善通脉灵胶囊质量控制标准。方法：采用薄层色谱法分别对通脉灵胶囊处方中丹参、乳香、没药、降香、川芎进行鉴别；对通脉灵胶囊的质量控制标准进行初步研究。结果：建立了操作简便，色谱斑点清晰，空白无干扰，易分辨的薄层定性方法。结论：通脉灵胶囊具有可控的质量标准。     

大七厘胶囊中松香酸补充检验方法研究

目的建立大七厘胶囊中非法添加物质松香酸的检查方法。方法采用薄层色谱法初步检测、再运用高效液相色谱-二极管阵列检测器进行验证。结果松香酸的测定范围在0~53.52μg/mL,呈良好的线性关系,r=0.998,平均回收率为100.4%,RSD为3.2%。结论所建立的方法准确可靠,操作简单,可用于大七厘胶囊中松香酸的定性及定量研究。     

玄麦胶囊中玄参麦冬桔梗的显微薄层鉴别

目的：根据中医药理论，结合现代临床医学研究，研制治疗慢性喉炎的玄麦胶囊。方法：用显微和薄层色谱鉴别控制质量。结果：方法简便，专属性强。结论：通过对处方中主药用显微和薄层色谱鉴别，可有效的控制“玄麦胶囊”质量。     

薄层扫描法测定跌打七厘片中血竭素的含量

目的　采用薄层扫描法测定跌打七厘片中血竭素的含量。方法　样品经适当提取、净化后点于硅胶 G薄层板上 ,氯仿 -甲醇 (19∶ 1)为展开剂 ,双波长反射法锯齿扫描 ,检测波长为 λs=480 nm,λR=5 6 0 nm。结果　本法线性关系良好 ,平均加样回收率为 96 .2 %,RSD值为 2 .4%。测得跌打七厘片中血竭素的含量约为 0 .0 38%。结论　本方法操作简单 ,准确 ,可用于跌打七厘片的质量控制。     

晶珠糖尿康胶囊的质量标准研究

目的：为控制晶珠糖尿康胶囊质量，建立藏茜草，小檗皮，诃子的薄层色谱（TCL）鉴别及盐酸小檗碱的薄层扫描定量方法，方法：采用TCL进行定性鉴别，用薄层扫描法进行含量测定。结果：鉴别方法专属性强，定量方法简便，准确，平均回收率为98.5%,RSD为1.08%，结论：本质量标准可有效地控制晶珠糖尿康胶囊质量。     

白癜风胶囊1号的薄层色谱鉴别研究

目的：建立白癜风胶囊1号的薄层色谱鉴别方法，为制定其质量控制标准提供试验依据。方法：采用薄层色谱鉴别法鉴别处方中的主要药味。结果：处方中的当归、川芎、牡丹皮、补骨脂、赤芍五味药的薄层色谱具有鉴别特征。结论：薄层色谱鉴别方法简便可靠，专属性、重观性好，可作为白癜风胶囊1号的质量控制指标。     

健脑益智胶囊的薄层色谱鉴别研究

目的：建立健脑益智胶囊的质量检测方法。方法：用薄层色谱法对该胶囊剂中的丹参、何首乌、当归、五味子进行了鉴别。结果：薄层色谱中斑点清晰，易于识别。结论：该方法可有效地控制健脑益智胶囊的质量。     

微波消解-电感耦合等离子体质谱法测定脉络宁注射液中25种矿物质元素

目的建立微波消解-电感耦合等离子体质谱(ICP-MS)直接稀释测定脉络宁注射液中25种矿物质元素(Mg、Ca、Fe、Cu、Zn、Mn、Al、B、Ba、Co、Cr、K、Li、Mo、Na、Ni、P、Pb、Sr、Th、Ti、V、As、Cd和Hg)的方法。方法分别对微波消解条件和测试条件进行考察;样品经微波消解后,采用电感耦合质谱仪测定25种矿物质元素,并对测定方法学进行考察。结果确定最佳消解条件为3步缓慢升温:400 W 80℃升温10 min,保留5 min;600 W 120℃升温10 min,保留5 min;900 W 200℃升温20 min,保留20 min;25种矿物质元素在各自的线性范围内线性关系良好,r≥0.999 6,精密度、稳定性和重复性试验的RSD均符合定量分析要求;加标回收率为94.7%~106.1%,RSD在0.34%~2.79%。脉络宁注射液中检测出Mg、Ca、Fe、Cu、Zn、Mn、Al、B、Ba、Co、Cr、K、Li、Mo、Na、Ni、P、Pb、Sr、Th、Ti、V,未检出As、Cd和Hg。结论该方法简便、迅速、准确,适用于脉络宁注射液中25种矿物质元素的同时测定。     

Die Lateralität und Lateralitätsinstabilität in der Diagnostik und Therapie

The disturbance and instability of laterality are obstacles to diagnostics and therapy. Correction prior to starting therapy is required. They also predispose toward defined health problems and unspecific diseases. Numerous research activities provide evidence of the relevance of undisturbed laterality in diagnostics and therapy. Techniques of testing and therapeutic corrections will allow for optimized therapy success.     

基于ICP-MS法的加味左金丸中无机元素分析

目的 通过电感耦合等离子体质谱（inductively coupled plasma mass spectrometry,ICP-MS）法建立加味左金丸中Cd、Pb、As、Hg、Co、V、Ni、Cu、Li、Sb、Ba、Mo、Sn、Cr、Na、Mg、Al、Ca、Ti、Mn、Fe、Zn、Ga、Se、Sr、Tl共计26种无机元素的测定方法。方法 加味左金丸通过微波消解法处理后,根据相对分子质量的大小选择内标物,其中⁷Li、²³Na、²⁴Mg、²⁷Al、⁴⁰Ca、⁴⁸Ti、⁵¹V、⁵²Cr、⁵⁵Mn、⁵⁶Fe、⁵⁸Ni、⁵⁹Co、⁶³Cu、⁶⁶Zn、⁷⁰Ga、⁷⁵As、⁷⁷Se、⁸⁶Sr以⁷²Ge作为内标;⁹⁵Mo、¹¹⁴Cd、¹¹⁸Sn、¹²¹Sb、¹³⁷Ba以¹¹⁵In作为内标;²⁰²Hg、²⁰⁵Tl、²⁰⁸Pb以²⁰⁹Bi作为内标。对标准品溶液、空白溶液与供试品溶液进行分析,采用标准曲线法进行定量分析。通过ICP-MS法进行测定。结果 26种无机元素线性的相关系数r ≥ 0.999 6,检出限为0.001~1.500μg/L,定量限为0.01~5.00 μg/L,精密度与重复性试验的RSD均小于5%,平均回收率在82.64%~106.44%,RSD均小于5%。对3个厂家的12批样品进行了测定,26种元素的含量差异较大,其中Na、Mg、Ca、Fe 4种元素的含量比较高,均大于500 μg/g,Cd、Pb、As、Hg、Co、Li、Sb、Mo、Sn、Cr、Se、Tl的含量比较低,均小于1 μg/g。由结果可知,人体的常量元素,如Na、Mg、Ca的含量比较高,Cd、Pb、As、Hg等有害元素含量比较低。根据《中国药典》2020年版一部的要求,本品中Cd、Pb、As、Hg与Cu均符合规定。结论 该方法快速、准确,可以用于加味左金丸中无机元素的测定。     

Erstaunliches Ergebnis einer Schädelakupunktur nach Yamamoto bei Hemihypsarrhythmie rechts

A girl, three and a half years old at the respective date, premature in 25th week of gestation, had been presented. On day three after birth, she had had a IVH III° right and left with severe involvement of parenchyma and other multiple complications, e. a. infant respiratory distress syndrome up to the 42nd day postpartum, and epileptic attacks with apnoeic events.     

Journal of Acupuncture and Tuina Science Instructions for Authors

The Journal of Acupuncture and Tuina Science, a journal with an international scope （IS SN 1672-3597, CN 31-1908/R, Bimonthly）, is embodied by ＇Springer Verlag＇ Database, Index Copernicus （IC） and Chinese Scientific and Technical Paper and Citations Data （CSTPCD）. You can search full text on http：//www, springerlink, com/content/1672 -3597.     

Yerba Mate or Paraguay Tea

正Beverages based on Ilex paraguariensis A.St.-Hil.are used in the south Brazil and other Latin American countries located at the so-called southern cone.It is known as chimarro or mate in south and southeast Brazil,tererêin     

Ethnopharmacologic study of chinese rhubarb

This paper deals with an interdisciplinary study covering historic, botanical, phytochemical, pharmacological and clinical aspects of rhubarb and related species, to lay stress on the correlation between plant phylogeny, chemical constituents and purgative activity.

It was found that the official rhubarbs were exclusively restricted in the Sect. Palmata e.g. Rheum palmatum R. palmatum var. tanguticum R. officinale; the following criteria may serve as their standard, viz., the presence of sennoside derivatives and rhein, the occurrence of the reduced form of rhein and aloe-emodin, the leaves with any kind of palmate incision. Comprehensive multivariate analyses showed that there is a very close relationship between the leaf incision, existence of sennosides or rhein and purgative activity.     

七味红花殊胜散对缺血再灌注肝损伤的保护作用

目的::研究七味红花殊胜敬对缺血再灌注肝损伤的保护作用.方法:在大鼠肝缺血再灌注模型上,观察七味红花殊胜散对缺血再灌注肝损伤引起的血清丙二醛(MDA)、超氧化物歧化酶(SOD)、谷胱甘肽过氧化物酶(GSH-Px)、一氧化氮(NO)含量的变化.结果:七味红花殊胜散对大鼠血清MDA、SOD、GSH与再灌组比较有明显差异(P<0.05),NO含量与再灌组比较有明显差异(P<0.05).结论:七味红花殊胜散对大鼠急性缺血再灌注肝损伤具有保护作用.     

Wirksamkeit der Akupunktur bei der Therapie von idiopathischen Schmeckstörungen: Eine randomisierte Placebo-kontrollierte Studie

Background

At present, the state-of-the-art medication in treating idiopathic taste disorder (gustatory dysfunction) is zinc. If zinc medication was unsuccessful, not tolerated or if it is contraindicated the persons affected can hardly be helped.

Objectives

In a randomized placebo-controlled clinical trial an attempt was made to determine the efficacy of acupuncture.

Methods

The treatment group was treated with acupuncture needles, the placebo group with an inactive acupuncture-laser. Endpoints of the study were changes in the taste test, the quality of life and the severity of symptoms of depression (BDI) as well as mood changes (ZMS). Satisfaction with the success of the respective therapy was also evaluated. Data were collected before and after therapy and again for the treatment group 10 weeks after completion of the treatment period.

Findings

Treatment with real acupuncture showed a significant improvement in gustatory function as well as a significant improvement in psychological symptoms. Greater satisfaction with the treatment results was evident in the treatment group. The treatment results of acupuncture remained stable over a period of ten weeks after completion of the treatment.

Conclusion

Acupuncture was effective in the therapy of idiopathic taste disorders and therefore it is an effective alternative when zinc medication is not tolerated or unsuccessful. But it is also suitable as a therapy of first choice. Acupuncture can be considered as an extension of the therapeutic spectrum in the difficult treatment of taste disorders.