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目的 建立宜肝乐颗粒的定性、定量鉴别方法 .方法 采用薄层色谱法对宜肝乐颗粒中鸡矢藤、功劳木、虎杖进行定性鉴别;高效液相色谱法测定宜肝乐颗粒中大黄素,Zorbax C18色谱柱(150 mm×4.6 mm,5 μm);流动相:甲醇-0.1%磷酸溶液(80 :20);检测波长:288 nm;体积流量:1.0 mL/min;柱温:室温;进样量:10μL.在此色谱条件下,理论塔板数按大黄素峰计达3 000以上,分离度为2.0.结果 3味药材的薄层色谱鉴别呈阳性;建立的定量测定方法 可用于宜肝乐颗粒中大黄素的测定.结论 薄层色谱法和高效液相色谱法简便、准确、灵敏,可作为宜肝乐颗粒质量控制的有效方法 . 相似文献
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驱风药酒质量标准研究 总被引:3,自引:0,他引:3
目的:建立驱风药酒(当归、川芎、陈皮、甘草、虎杖等)质量标准.方法:采用薄层色谱法对驱风药酒中的当归、川芎、陈皮、甘草、虎杖进行了定性鉴别;并应用双波长薄层扫描法对虎杖中有效成分大黄素的含量进行测定.结果:本法平均加样回收率为99.2%、RSD为0.74%.结论:本法操作简单,重现性好,可作为驱风药酒质量控制. 相似文献
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目的 :甘露消渴胶囊定性定量方法研究。 方法 :采用薄层色谱法(TLC)对处方中人参、枸杞子、麦冬进行了定性鉴别;采用高效液相色谱法对方中小檗碱进行了含量测定。 结果 :TLC定性鉴别能检出人参、枸杞子、麦冬,薄层色谱特征明显,专属性强,且阴性无干扰; HPLC测定小檗碱在0.0463~0.3804 μg线性关系良好,平均回收率99.14%,RSD 0.98%(n=6)。 结论 :薄层色谱鉴别和含量测定方法准确可行,重复性好,能有效地控制甘露消渴胶囊的质量。 相似文献
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目的:建立朱砂七的质量标准。方法:建立朱砂七的薄层色谱定性方法,并对其主要成分大黄素进行定量控制,色谱条件为HypersilC18柱(4.6mm×250mm,5μm),甲醇-水-磷酸(85:15:0.01)为流动相,流速1.0ml.min-1,柱温30℃,检测波长254nm。结果:薄层鉴别检出虎杖苷,含量测定中大黄素峰与其它峰分离良好,在0.0226~0.2825μg范围内呈良好的线性关系,加样回收率为99.8%,RSD=1.8%(n=5)。结论:通过薄层色谱法对朱砂七进行鉴别,高效液相色谱法测定主成分大黄素的含量,建立朱砂七完善的质量标准,作为对朱砂七质量控制的依据。 相似文献
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目的:建立朱砂七的质量标准。方法:建立朱砂七的薄层色谱定性方法,并对其主要成分大黄素进行定量控制,色谱条件为HypersilC18柱(4.6mm×250mm,5μm),甲醇-水-磷酸(85:15:0.01)为流动相,流速1.0ml.min-1,柱温30℃,检测波长254nm。结果:薄层鉴别检出虎杖苷,含量测定中大黄素峰与其它峰分离良好,在0.0226~0.2825μg范围内呈良好的线性关系,加样回收率为99.8%,RSD=1.8%(n=5)。结论:通过薄层色谱法对朱砂七进行鉴别,高效液相色谱法测定主成分大黄素的含量,建立朱砂七完善的质量标准,作为对朱砂七质量控制的依据。 相似文献
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目的建立微波消解-电感耦合等离子体质谱(ICP-MS)直接稀释测定脉络宁注射液中25种矿物质元素(Mg、Ca、Fe、Cu、Zn、Mn、Al、B、Ba、Co、Cr、K、Li、Mo、Na、Ni、P、Pb、Sr、Th、Ti、V、As、Cd和Hg)的方法。方法分别对微波消解条件和测试条件进行考察;样品经微波消解后,采用电感耦合质谱仪测定25种矿物质元素,并对测定方法学进行考察。结果确定最佳消解条件为3步缓慢升温:400 W 80℃升温10 min,保留5 min;600 W 120℃升温10 min,保留5 min;900 W 200℃升温20 min,保留20 min;25种矿物质元素在各自的线性范围内线性关系良好,r≥0.999 6,精密度、稳定性和重复性试验的RSD均符合定量分析要求;加标回收率为94.7%~106.1%,RSD在0.34%~2.79%。脉络宁注射液中检测出Mg、Ca、Fe、Cu、Zn、Mn、Al、B、Ba、Co、Cr、K、Li、Mo、Na、Ni、P、Pb、Sr、Th、Ti、V,未检出As、Cd和Hg。结论该方法简便、迅速、准确,适用于脉络宁注射液中25种矿物质元素的同时测定。 相似文献
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O. Mastalier 《Deutsche Zeitschrift für Akupunktur (in deutscher Sprache / in German)》2013,56(4):26-29
The disturbance and instability of laterality are obstacles to diagnostics and therapy. Correction prior to starting therapy is required. They also predispose toward defined health problems and unspecific diseases. Numerous research activities provide evidence of the relevance of undisturbed laterality in diagnostics and therapy. Techniques of testing and therapeutic corrections will allow for optimized therapy success. 相似文献
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正Beverages based on Ilex paraguariensis A.St.-Hil.are used in the south Brazil and other Latin American countries located at the so-called southern cone.It is known as chimarro or mate in south and southeast Brazil,tererêin 相似文献
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Chen Han-ping 《针灸推拿医学(英文版)》2014,(5):I0003-I0004
The Journal of Acupuncture and Tuina Science, a journal with an international scope (IS SN 1672-3597, CN 31-1908/R, Bimonthly), is embodied by 'Springer Verlag' Database, Index Copernicus (IC) and Chinese Scientific and Technical Paper and Citations Data (CSTPCD). You can search full text on http://www, springerlink, com/content/1672 -3597. 相似文献
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This paper deals with an interdisciplinary study covering historic, botanical, phytochemical, pharmacological and clinical aspects of rhubarb and related species, to lay stress on the correlation between plant phylogeny, chemical constituents and purgative activity.
It was found that the official rhubarbs were exclusively restricted in the Sect. Palmata e.g. Rheum palmatum R. palmatum var. tanguticum R. officinale; the following criteria may serve as their standard, viz., the presence of sennoside derivatives and rhein, the occurrence of the reduced form of rhein and aloe-emodin, the leaves with any kind of palmate incision. Comprehensive multivariate analyses showed that there is a very close relationship between the leaf incision, existence of sennosides or rhein and purgative activity. 相似文献
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目的 通过电感耦合等离子体质谱(inductively coupled plasma mass spectrometry,ICP-MS)法建立加味左金丸中Cd、Pb、As、Hg、Co、V、Ni、Cu、Li、Sb、Ba、Mo、Sn、Cr、Na、Mg、Al、Ca、Ti、Mn、Fe、Zn、Ga、Se、Sr、Tl共计26种无机元素的测定方法。方法 加味左金丸通过微波消解法处理后,根据相对分子质量的大小选择内标物,其中7Li、23Na、24Mg、27Al、40Ca、48Ti、51V、52Cr、55Mn、56Fe、58Ni、59Co、63Cu、66Zn、70Ga、75As、77Se、86Sr以72Ge作为内标;95Mo、114Cd、118Sn、121Sb、137Ba以115In作为内标;202Hg、205Tl、208Pb以209Bi作为内标。对标准品溶液、空白溶液与供试品溶液进行分析,采用标准曲线法进行定量分析。通过ICP-MS法进行测定。结果 26种无机元素线性的相关系数r ≥ 0.999 6,检出限为0.001~1.500μg/L,定量限为0.01~5.00 μg/L,精密度与重复性试验的RSD均小于5%,平均回收率在82.64%~106.44%,RSD均小于5%。对3个厂家的12批样品进行了测定,26种元素的含量差异较大,其中Na、Mg、Ca、Fe 4种元素的含量比较高,均大于500 μg/g,Cd、Pb、As、Hg、Co、Li、Sb、Mo、Sn、Cr、Se、Tl的含量比较低,均小于1 μg/g。由结果可知,人体的常量元素,如Na、Mg、Ca的含量比较高,Cd、Pb、As、Hg等有害元素含量比较低。根据《中国药典》2020年版一部的要求,本品中Cd、Pb、As、Hg与Cu均符合规定。结论 该方法快速、准确,可以用于加味左金丸中无机元素的测定。 相似文献
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H. Brandt B. Hauswald H. Langer J. Gleditsch Th. Zahnert 《Deutsche Zeitschrift für Akupunktur (in deutscher Sprache / in German)》2008
Background
At present, the state-of-the-art medication in treating idiopathic taste disorder (gustatory dysfunction) is zinc. If zinc medication was unsuccessful, not tolerated or if it is contraindicated the persons affected can hardly be helped.Objectives
In a randomized placebo-controlled clinical trial an attempt was made to determine the efficacy of acupuncture.Methods
The treatment group was treated with acupuncture needles, the placebo group with an inactive acupuncture-laser. Endpoints of the study were changes in the taste test, the quality of life and the severity of symptoms of depression (BDI) as well as mood changes (ZMS). Satisfaction with the success of the respective therapy was also evaluated. Data were collected before and after therapy and again for the treatment group 10 weeks after completion of the treatment period.Findings
Treatment with real acupuncture showed a significant improvement in gustatory function as well as a significant improvement in psychological symptoms. Greater satisfaction with the treatment results was evident in the treatment group. The treatment results of acupuncture remained stable over a period of ten weeks after completion of the treatment.Conclusion
Acupuncture was effective in the therapy of idiopathic taste disorders and therefore it is an effective alternative when zinc medication is not tolerated or unsuccessful. But it is also suitable as a therapy of first choice. Acupuncture can be considered as an extension of the therapeutic spectrum in the difficult treatment of taste disorders. 相似文献19.
A girl, three and a half years old at the respective date, premature in 25th week of gestation, had been presented. On day three after birth, she had had a IVH III° right and left with severe involvement of parenchyma and other multiple complications, e. a. infant respiratory distress syndrome up to the 42nd day postpartum, and epileptic attacks with apnoeic events. 相似文献
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