| 香青兰化学成分的研究 |
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| 引用本文： | 古海锋,陈若芸,孙玉华,刘发.香青兰化学成分的研究[J].中国中药杂志,2004,29(3):232-234. |
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| 作者姓名： | 古海锋 陈若芸 孙玉华 刘发 |
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| 作者单位： | 1. 中国医学科学院,中国协和医科大学,药物研究所,北京,100050
2. 新疆维吾尔自治区药物研究所,新疆,乌鲁木齐,830002 |
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| 摘 要： | 目的 :研究香青兰全草的化学成分。方法 :利用RA型大孔树脂 ,聚酰胺和硅胶色谱技术进行分离纯化 ,根据理化性质及各种光谱技术进行结构鉴定。结果 :香青兰乙醇提取物经大孔树脂柱色谱 ,从 50 %乙醇洗脱部分得到 8个化合物 ,分别鉴定为洋芹素 (apigenin ,Ⅰ ) ,木犀草素 (luteolin ,Ⅱ ) ,山柰酚 (kaempferol ,Ⅲ ) ,异鼠李素(isorhamnetin ,Ⅳ ) ,田蓟苷 (tilianin ,Ⅴ ) ,agastachoside (Ⅵ ) ,acacetin 7O(6 O malonyl β D glucopyranoside ,Ⅶ )和丁香脂素 (syringaresinol,Ⅷ )。结论 :化合物Ⅳ ,Ⅶ和Ⅷ为首次从该属植物中分离得到 ,化合物Ⅰ ,Ⅱ和Ⅲ为首次从该植物中分离得到。
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| 关 键 词： | 香青兰 田蓟苷 异鼠李素 丁香脂素 acacetin-7-O(6-Omalonyl-β-D-glucopyranoside) |
| 文章编号： | 1001-5302(2004)03-0232-03 |
| 收稿时间： | 2003/4/20 0:00:00 |
Studies on chemical constituents from herb of Dracocephalum moldavica |
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| GU Hai-feng ;CHEN Ruo-yun ;SUN Yu-hua ;LIU Fa.Studies on chemical constituents from herb of Dracocephalum moldavica[J].China Journal of Chinese Materia Medica,2004,29(3):232-234. |
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| Authors: | GU Hai-feng ;CHEN Ruo-yun ;SUN Yu-hua ;LIU Fa |
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| Affiliation: | Institute of Materia Medica, Chinese Academy of Medical Sciences, Beijing 100050, China. |
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| Abstract: | OBJECTIVE: To study the chemical constituents from the whole plant of Dracocephalum moldavica. METHOD: The compounds were isolated by using column chromatography with RA polystyrene resin, polyamide and silica gel as packing materials, and the structures of the compounds were identified by means of spectral data. RESULT: eight compounds were identified as apigenin(I), luteolin(II), kaempferol(III), isorhamnetin(IV), tilianin(V), agastachoside(VI), acacetin-7-O-(6-O-Malonyl-beta-D-glucopyranoside) (VII) and syringaresinol(VIII). CONCLUSION: Compounds I, II and III were isolated from genus Dracocephalum for the first time and compounds IV, VII and VIII were isolated from Dracocephalum moldavuca for the first time. |
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