| 柴胡微波辅助提取工艺研究 |
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| 引用本文： | 李棣华,刘俊红,伍孝先,吕沅珊. 柴胡微波辅助提取工艺研究[J]. 天津中医药大学学报, 2012, 29(3): 289-291 |
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| 作者姓名： | 李棣华 刘俊红 伍孝先 吕沅珊 |
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| 作者单位： | 天津市中西医结合急腹症研究所药物研究室, 天津 300100;天津市中西医结合急腹症研究所药物研究室, 天津 300100;天津市中西医结合急腹症研究所药物研究室, 天津 300100;天津市中西医结合急腹症研究所药物研究室, 天津 300100 |
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| 基金项目： | 天津市卫生局中医、中西医结合科研课题(07017). |
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| 摘 要： | [目的] 优化微波提取柴胡有效成分的最佳工艺条件。[方法] 以常规回流提取正交结果为基准,采用HPLC对柴胡皂苷成分进行监测,优化柴胡微波提取的各影响因素。[结果] 优选柴胡提取工艺为微波功率800 W,以50%乙醇,每次8倍量,提取3次,每次20 min.[结论] 表明微波提取技术法的提取时间短,效率高,优于常规回流提取方法。
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| 关 键 词： | 柴胡 柴胡皂苷a、d 微波辅助提取 |
| 收稿时间： | 2012-01-09 |
Technical study on microwave-assisted extraction from Radix Bupleuri |
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| LI Di-hu,LIU Jun-hong,WU Xiao-xian and LV Yuan-shan. Technical study on microwave-assisted extraction from Radix Bupleuri[J]. Journal of Tianjin University of Traditonal Chinese Medicine, 2012, 29(3): 289-291 |
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| Authors: | LI Di-hu LIU Jun-hong WU Xiao-xian LV Yuan-shan |
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| Affiliation: | Department of Medical Research, Tianjin Institute of Acute Abolominal Diseases of Integrated Traditional Chinese and Westen Medicine, Tianjin 300100, China;Department of Medical Research, Tianjin Institute of Acute Abolominal Diseases of Integrated Traditional Chinese and Westen Medicine, Tianjin 300100, China;Department of Medical Research, Tianjin Institute of Acute Abolominal Diseases of Integrated Traditional Chinese and Westen Medicine, Tianjin 300100, China;Department of Medical Research, Tianjin Institute of Acute Abolominal Diseases of Integrated Traditional Chinese and Westen Medicine, Tianjin 300100, China |
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| Abstract: | [Objective] To optimize the technological conditions for the exaction of effective compounds from Bupleurum Chinese DC. by microwave-assisted art. [Methods] Taking the results of the routine backflow extraction optimized by an orthogonal test as the standard and using HPLC for monitoring the contents of saikosaponin the influence factors for microwave-assisting extraction from Radix Bulpleuri were optimized. [Results] The optimized extractions conditions were: to set the microwave power rate at 800 W; to exact three times with eight times volume of ethyl alcohol for 20 min each time. [Conclusion] The technique with microwave extraction is better than the method of backflow extraction with high efficiency and short extraction time. |
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